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Beilstein J. Org. Chem. 2021, 17, 813–818, doi:10.3762/bjoc.17.70
Graphical Abstract
Scheme 1: Retrosynthesis of compound 1.
Scheme 2: Reported bis(aryloxy)fluoromethane syntheses. Reagents and conditions: (a) Cl2FCH, NaOH, 1,4-dioxan...
Scheme 3: Attempted synthesis of 4. Reagents and conditions: (a) Ca(OH)2, 1,4-dioxane/water, reflux, 72 h, 5%...
Scheme 4: Synthesis of 10. Reagents and conditions: (a) BrFCHCO2Et, Cs2CO3, DMF, 35 °C, 16 h then H2O, 35 °C,...
Scheme 5: Synthesis of 1. Reagents and conditions: (a) 1,3-dibromo-5,5-dimethylhydantoin, benzoyl peroxide, (...
Scheme 6: Synthesis of 11–13. Reagents and conditions: ArOH (1.3 mmol), Br2FCH (1.3 mmol), KOH (4 mmol), MeCN...
Scheme 7: Proposed mechanism for the formation of compound 11.